Autoindex 後、Predict で解の妥当性を確認後 Main menu の Strategy をク リックすることで、STRATEGY がスタートする。まず、必要な撮影範囲を見積 もる。
数行の説明の後、以下のような表示になる。 Do you want to proceed (Y): MOSFLM =>strategy ! 標準モードで実行する Running strategy in default mode. Type GO to continue or ABORT to stop. MOSFLM =>go SPEEDUP factor set to 27.0 Angles between a axis and X,Y,Z axes 105.233 107.633 156.360 Angles between b axis and X,Y,Z axes 82.271 162.114 73.972 Angles between c axis and X,Y,Z axes 162.833 92.904 73.095 The a axis is closest to the rotation axis (angle 23.64) Rotation angle to get the b axis in XZ plane 81.96 Rotation angle to get the c axis in XZ plane -3.03 Unique axis is: c Rotation angle to get the unique axis into the YZ plane: 267.0 Generating reflection list Generated reflections for phi range -123.0 to -18.0 Sorting the generated list. Generating the list of unique reflections. Merging the generated and unique reflection list. Checking completeness of data <- この結晶は cubic Optimum rotation gives 95.5% of unique data. <- なので、247度から This corresponds to the following rotation range(s): <- 292度の範囲を測定 From 247.0 to 292.0 degrees <- すれば 95.5% となる。 Type "STATS" at prompt for full statistics.